JAWAHARLAL NEHRU TECHNOLOGICAL UNIVERSITY HYDERABAD

Overview

I Experiments involving laboratory techniques Recrystallization Steam distillation

II Determination of following oil values (including standardization of reagents) Acid value Saponification value Iodine value

III Preparation of compounds

• Benzanilide/Phenyl benzoate/Acetanilide from Aniline/ Phenol /Aniline by acylation reaction.
• 2,4,6-Tribromo aniline/Para bromo acetanilide from Aniline/ Acetanilide by halogenation (Bromination) reaction.
• 5-Nitro salicylic acid/Meta di nitro benzene from Salicylic acid / Nitro benzene by nitration reaction.
• Benzoic acid from Benzyl chloride by oxidation reaction.
• Benzoic acid/ Salicylic acid from alkyl benzoate/ alkyl salicylate by hydrolysis reaction.
• 1-Phenyl azo-2-napthol from Aniline by diazotization and coupling reactions.
• Benzil from Benzoin by oxidation reaction.
• Dibenzal acetone from Benzaldehyde by Claison Schmidt reaction
• Cinnammic acid from Benzaldehyde by Perkin reaction
• P-Iodo benzoic acid from P-amino benzoic acid Recommended Books (Latest Editions)
• 1. Organic Chemistry by Morrison and Boyd
• 2. Organic Chemistry by I.L. Finar , Volume-I
• 3. Textbook of Organic Chemistry by B.S. Bahl & Arun Bahl.
• 4. Organic Chemistry by P.L.Soni
• 5. Practical Organic Chemistry by Mann and Saunders.
• 6. Vogel’s text book of Practical Organic Chemistry
• 7. Advanced Practical organic chemistry by N.K.Vishnoi.
• 8. Introduction to Organic Laboratory techniques by Pavia, Lampman and Kriz.