JAWAHARLAL NEHRU TECHNOLOGICAL UNIVERSITY HYDERABAD

Course Objectives

To introduce spectroscopic methods, Chemical Instrumental Analysis,

Electro-analytical methods to numerous applications ranging across healthcare, environmental, and pharmaceutical industries.

Course Outcomes

The student is expected to acquire the knowledge is instruments used in

Pharma and chemical Industries.

UNIT - I

pH and Conductivity & Dissolved Component Analyzer: Conductivity meters – pH meters – Dissolved oxygen, hydrogen analyzers – Sodium analyzer – Silica analyzer and sampling systems. Gas Analyzers: Thermal conductivity types – CO monitor – NOX analyzer – H 2 S analyzer system and sampling – Industrial analyzer circuits, Theory and problems on Beer – Lamberts Law.

UNIT - II

Chromatography – I: Gas chromatography – Liquid chromatography – their principles and applications. Chromatography – II: Oxygen analyzer – paramagnetic type – detectors and sampling systems.

UNIT - III

Spectrophotometers – I: UV, VIS Spectrophotometers – Single beam and double beam instruments – Instrumentation associated with the above Spectrophotometers – Sources and detectors – Sources and detectors for IR Spectrophotometers.

UNIT - IV

Spectrophotometers – II: FT IR Spectrometer – Flame emission and atomic absorption Spectrophotometer – Atomic emission Spectrophotometer - sources for Flame Photometers and online calorific value measurements.

UNIT - V

Principle of Nuclear Magnetic Resonance: Instrumentation associated with NMR Spectrophotometer – Introduction to mass spectrophotometers, Principle, and brief discussion on ELECTRON SPIN RESONANCE (ESR.) Special Analytical Instruments: Nuclear radiation detectors – Ionization chamber – GM Counter – Proportional Counter – Solid state detectors ND PMT.

R16 B.TECH EIE.

TEXT BOOKS:

• 1. Handbook of Analytical Instruments – by Khandpur. TMH.
• 2. Analytical Instrumentation by Bela G. Liptak, CRC Press -1994.

REFERENCE BOOKS:

• 1. Instrumental Methods of Analysis – by Willard H.H., Merrit L.L., Dean J.A.and Seattle F.L., CBS Publishing and Distributors, 6/e, 1995.
• 2. Instrument Technology – by Jones B.E., Butterworth Scientific Publ., London, 1987.
• 3. Mechanical and Industrial Measurements – by Jain R.K., Khanna Publishing, New Delhi, 2/e, 1992.
• 4. Principles of Instrumental Analysis – by Skoog D.A. and West D.M., Holt Sounder Publication, Philadelphia, 1985.
• 5. Instrumental Analysis – by Mann C.K., Vickerks T.J. & Gullick W.H., Harper and Row Publishers, New York, 1974. R16 B.TECH EIE.