JAWAHARLAL NEHRU TECHNOLOGICAL UNIVERSITY HYDERABAD

JAWAHARLAL NEHRU TECHNOLOGICAL UNIVERSITY HYDERABAD B.Pharmacy I Year PHARMACEUTICAL ANALYSIS-I Previous Question Paper (July-2021 - R17)

B.Pharmacy | I Year | I-I | R17 | July-2021

Answer PaperPaper Code: 241ABMaximum Marks: 75Time: 3hours

Answer any five questions

All questions carry equal marks

Main

115 marks
a

Accuracy

5 marks

Answer

Accuracy refers to the closeness of a measured value to the true or accepted reference value. It is a measure of the correctness of an analytical result. Accuracy is typically expressed in terms of absolute error or relative error. It is influenced by systematic errors, which cause a consistent deviation from the true value. Improving accuracy involves calibration of instruments, use of standard reference materials, and performing blank determinations to eliminate bias.

b

Precision

5 marks

Answer

Precision describes the degree of agreement or reproducibility between replicate measurements of the same quantity. It indicates the random variation in a set of results and is independent of the true value. Precision is commonly expressed statistically using standard deviation, variance, or the coefficient of variation (relative standard deviation). High precision implies that repeated measurements yield very similar results, though these results may still be inaccurate if a systematic error is present.

c

Types of errors

5 marks

Answer

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2

Explain in detail the preparation and standardization procedure and principle of the following:

15 marks
a

Sodium hydroxide

8 marks

Answer

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b

Sulphuric acid

7 marks

Answer

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3

Write a detailed note on the different types of neutralization curves for acid-base titrations.

15 marks

Answer

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4

Explain in detail with suitable examples the principle involved in non-aqueous titration.

15 marks

Answer

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5

Explain the following in detail with examples

15 marks
a

Mohr's method

7 marks

Answer

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b

Fajans method

8 marks

Answer

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6

Explain in detail the steps involved in gravimetric titration.

15 marks

Answer

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7

Explain in detail the principle involved and applications of Bromatometry titration with any two examples of compounds estimated by Bromatometry.

15 marks

Answer

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8

Write a note on the following:

15 marks
a

Principle involved in Polarography

8 marks

Answer

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b

Applications of Polarography

7 marks

Answer

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About this paper

This page contains the solved question paper with answers of PHARMACEUTICAL ANALYSIS-I from JAWAHARLAL NEHRU TECHNOLOGICAL UNIVERSITY HYDERABAD for B.Pharmacy I Year I-I, July-2021, R17.

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